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الموضوع العلمي |
عدد الساعات |
محاضرة |
تمارين |
مناقشة |
مذاكرة مستقلة |
الاسبوع |
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Gravimetric analysis Examples of Gravimetric Analysis Advanced Problems) Precipitation Colloids and Dialysis Examples of Gravimetric Calculations Combustion Analysis Thermogravimetric analysis Instrumentation
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CHEMICAL EQUILIBRIA Aqueous Solutions and Chemical Equilibria Effect of Electrolytes on Chemical Equilibria Equilibrium Problems for Complex Systems 1. Activity and the Systematic Treatment of Equilibrium Opener: Hydrated Ions The Effect of Ionic Strength on Solubility of Salts Effect of Ionic Strength on Ion Dissociation Salts with Ions of Charge Activity Coefficients pH Revisited Systematic Treatment of Equilibrium Calcium Carbonate Mass Balance in Rivers Applying the Systematic Treatment of Equilibrium 2. Polyprotic Acid-Base Equilibria Diprotic Acids and Bases Carbon Dioxide in the Air and Ocean (new) Successive Approximations Polyprotic Acids and Bases Which Is the Principal Species? Fractional Composition Equations Isoelectric and Isoionic Dependence of Solubility on pH (Advanced Problems) Analyzing Acid-Base Titrations with Difference Plots (Advanced Problems) |
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3. The Need for Quality Assurance Basics of Quality Assurance Control Charts Method Validation The Horwitz Trumpet: Variation in Inter laboratory Precision Standard Addition Internal Standards Efficiency in Experimental Design 4. Using Microsoft Excel in Advanced Analytical Chemistry Problems
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Principles of Chromatography Introduction to Chromatography What Is the Chromatographic Process Chromatography in More than One Dimension Visualization of the Chromatographic Process at the Molecular Level: Analogy to Basic Equations Describing Chromatographic Separations How Do Column Variables Affect Efficiency (Plate Height) 5. Practical Optimization of Chromatographic Separations Qualitative Chromatography: Analyte Identification Quantitative Measurements in Chromatography Peak Area or Peak Height: What Is Best for Quantitation Calibration with an External Standard Calibration with an Internal Standard Examples of Chromatographic Calculations |
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Gas Chromatography Historical Development of GC: The First Chromatographic Instrumentation Advances in GC Leading to Present-Day Instrumentation GC Instrument Component Design (Injectors) Syringes. Autosamplers SPME Split Injections Splitless Injections GC Instrument Component Design (the Column) Column Stationary Phase Selecting a Stationary Phase for an Application Effects of Mobile Phase Choice and Flow Parameters GC Instrument Component Design (Detectors) Hyphenated GC Techniques (GC-MS, GC-IR, GC-GC, or 2D GC Comprehensive 2D Gas Chromatography Retention Indices (A Generalization of Relative Rt Information) Scope of GC Analyses GC Behavior of Organic Compound Classes Derivatization of Difficult Analytes to Improve GC Elution Behavior |
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High-Performance Liquid Chromatography HPLC Column and Stationary Phase Support Particle Considerations Stationary-Phase Considerations. Chiral Phases for Separation of Enantiomers Effects on Separation of Composition of the Mobile Phase New HPLC-Phase Combinations for Assays of Very Ion-Exchange Chromatography. HPLC Detector Design and Operation Interfacing HPLC to Mass Spectrometry Applications of HPLC Chromatography of Ions Dissolved in Liquids Ion Chromatography Single-Column IC Indirect Detection in IC Affinity Chromatography Size-Exclusion Chromatography Supercritical Fluid Chromatography |
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6. Ultraviolet, Visible, I. Introduction II. Spectrophotometer Characteristics A. The Architecture of a Spectrophotometer III. Present and Future UV – VIS – NIR Spectrometers Instrumentation Practical and Applications |
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7. Atomic Absorption Spectrometry and Related Techniques I. Introduction A. AAS Graphite Furnace II. Atomic Spectra in Absorption, Emission, and Fluorescenc Spectrometers for AAS III. The Techniques of Atomic Spectrometry A. The FAAS Technique B. The GFAAS Technique Chemical Vapor Generation C. Spectrometers for AFS Spectrometers for Flame OES IV. Measurement, Calibration, and Evaluation in AAS, AFS, and OES A. Samples and Measurement Solution B. Calibration, Evalution ICP ICP-MS |
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NMR Introduction Instrument Design Magnet Systems B. NMR Probes C. RF Generation and Signal Detection D. Magnetic Field Gradients E. Computer Systems F. Accessories III. Theoretical Background Data Analysis and Interpretation |
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Mass Spectrometry Instrumentation V. Ionization Methods A. Matrix-Assisted Laser Desorption/Ionization B. Electrospray Ionizatio VI. Mass Analyzers A. Triple Quadrupole Mass Spectrometer Time of Flight Mass Spectrometer Data analysis and problems |
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