CH013 : Practical Analytical Chemistry (III)

Department

Department of Chemistry

Academic Program

Bachelor in Chemistry

Type

Compulsory

Credits

01

Prerequisite

CH212

Overview

The course aims to introduce the student to the following:• Knowledge of the theoretical foundations and principles of automated chromatographic analysis• Knowledge of the theoretical foundations and principles of automated spectral analysis of devices such as GC, HPLC, EP• Knowledge of theoretical calculations related to the work of these devices• Knowledge of the practical applications of these devices in various environmental analyzes• Preparation of various ion exchangers

Intended learning outcomes

a. Knowledge & understandingA.1 The student will be familiar with the theoretical foundations and principles of the instrumental analysis by chromatographic methodsA.2 Giving the student experience on the theoretical basis of the different methods of separationA.3 The ability to solve mathematical problems related to the work of these methodsA.4 Know the special applications of each method in qualitative and quantitative analysis and how to deal with them A.5 The student will know how to operate GC, HPLC, quality methods, results analysis and processingB. Mental skillsB.1 Analyze problems and apply technical solutions for chromatographic separation methodsB.2 Compare the different chapters in environmental analysisB.3 Analysis of results and data related to chromatography, different separation methods, and error handlingB.4 Participation in the research activity of the devicesB.5 Identify the defects and interferences related to the analysis of the devicesT. Practical & professional skillsC.1 Using some methods of chromatographic analysis in analyzing real samplesC.2 Designing practical experiments using GC, HPLC devicesC.3 Choose the appropriate separation method for the type of analysis in the laboratoryC.4 The ability to operate and maintain the devices, the skill of using the ISO, and following the appropriate separation methodC5 The ability to use mathematical and statistical methods to analyze the results obtained from these methodsw. Generic and transferable skillsD.1 presents the information and explains the work and installation of the equipment orally and in writingD.2 Using appropriate techniques for chromatographic analysis and other separation methods in analyzing real samplesD.3 Work individually and independently, relying on personal skills to understand, analyze and operate equipmentD.4 Discussion in a scientific mannerD.5 Be able to present data and write reports in proper language

Teaching and learning methods

1 . Lectures 2 . Duties 3 . Periodic tests

Methods of assessments

First written exam 25%Second written exam 25%final exam 50%

Scientific subject

The number of hours

a lecture

Lab

discussion

Independent study

number

weeks

1. Estimate the percentage of iodine extraction from an organic solvent

3

-

3

-

-

1

Extraction of iron(III) using solvent extraction and estimation spectrophotometrically

3

-

3

-

-

1

  1. Determination of lead spectrophotometrically by solvent extraction

3

-

3

-

-

1

  1. Determine the exchange capacity of cationic and anion exchangers

3

-

3

-

-

1

  1. Separation of zinc from magnesium using an anion exchanger

3

-

3

-

-

1

  1. Choosing the appropriate solvent to separate commercial ink by paper chromatography

3

-

3

-

-

1

  1. Commercial ink separation by paper chromatography

3

-

3

-

-

1

  1. Separation of orthonitrophenol from paranitrophenol by thin layer chromatography

3

-

3

-

-

1

  1. Testing the purity of acetylsalicylic acid using thin layer chromatography

3

-

3

-

-

1

  1. Separation of potassium permanganate solution from potassium dichromate solution by classical column chromatography

3

-

3

-

-

1

  1. Qualitative analysis of organic substances by gas chromatography

3

-

3

-

-

1

  1. Qualitative analysis of organic substances by gas chromatography

3

-

3

-

-

1

  1. Determining the concentration of caffeine in tea, coffee, and soft drinks using a high-efficiency liquid chromatography device

3

-

3

-

-

1

  1. Determine the concentration of bromate and phosphate in water using ion chromatography

3

-

3

-

-

1

  1. Using an electrophoresis device to separate a specific protein

3

-

3

-

-

1

1. the reviewer (References)

References title

publisher

Release

Author

Her whereabouts

Chromatography: Concepts and Contrasts,

Wiley

2nd edition

James M. Millerr

Internet

Advances in chromatography

CRC

Volume 65

Fli

Science Library - Internet

Undergraduate Instrumental Analysis

CRC Press

7th edition

James W. Robinson, Eileen Skelly Frame, George M. Frame II

Science Library - Internet

websites

https://Chemistry.com.pk

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Arabic language 1 (AR051)
General Physics І (Electricity ) (PH110)
General Chemistry 1 (CH101)
Mathematics 1 (MA100)
English Language 1 (EL101)
Principles of Atmospheric Science (AT112)
General Physics 2 (PH112)
General chemistry 2 (CH102)
General Chemistry 2 Laboratory (CH103)
Calculus and Analysis principle 2 (MA102)
Organic chemistry I (CH231)
Thermodynamics and Gases (CH241)
Ordinary Differential Equations (MA201)
Fundamentals of Inorganic Chemistry (CH221)
Analytical Chemistry(I) (CH211)
Practical Analytical Chemistry (CH213)
Methods for preparing inorganic compounds I (practical) (CH223)
Organic chemistry II (CH232)
Practical Analytical Chemistry, (CH214)
Thermodynamics and solutions (CH242)
Chemistry of Main Group Elements (CH222)
Analytical Chemistry(II) (CH212)
English language 2 (EL102)
Practical Analytical Chemistry (III) (CH013)
Organic chemistry Practical (CH031)
Industrial Chemistry (CH461)
Electrochemistry (CH341)
Thermodynamics and Solutions Lab (CH243)
Analytical Chemistry(III) (CH311)
Fundamentals of transition elements (CH321)
organic chemistry 3 (CH331)
Practical Industrial chemistry I (CH463)
Practical Analytical Chemistry(IV) (CH014)
Analytical Chemistry(IV) (CH312)
Transition elements chemistry studies (CH322)
Organic chemistry III Practical (CH333)
Biochemistry (CH451)
Organic chemistry IV (CH332)
Quantum chemistry (CH342)
Electrochemistry Lab (CH345)
Biochemistry lab I (CH453)
Molecular Spectroscopy (CH343)
Organic chemistry IV Practical (CH033)
Solid State Chemistry (CH344)
Practical Analytical Chemistry(V), (CH414)
Organometallic Chemistry (CH421)
Preparation and Methods for detection of inorganic compounds (CH424)
Industrial Chemistry (II) (CH462)
Analytical Chemistry(V) (CH441)
Nuclear chemistry (CH323)
Industrial Chemistry (II) Lab (CH464)
Kinetic Chemistry lab (CH043)
Kinetic Chemistry (CH442)