CH211 : Analytical Chemistry(I)

Department

Department of Chemistry

Academic Program

Bachelor in Chemistry

Type

Compulsory

Credits

02

Prerequisite

CH102

Overview

The course aims to introduce the student to the following:• Theoretical foundations and principles related to quantitative gravimetric and volumetric analysis.• Types of chemical reactions used in quantitative gravimetric and volumetric analysis.• Mathematical calculations related to quantitative gravimetric analysis, neutralization and sedimentation titrations.• How to prepare and discuss the results based on the technique used in the analysis.• How to determine the appropriate method for analyzing samples quantitatively by gravimetric analysis or titration.

Intended learning outcomes

a. Knowledge & understandingA.1 Understand the basic information related to gravimetric and volumetric quantitative analysis methodsA.2 Learn the basic concepts of the types of chemical reactions used in analysisA.3 Learn how to calculate the amount of a chemical and determine the concentration of solutions when doing a chemical analysis.A.4 Learn how to prepare and process results A.5 Understand how to choose the appropriate method for analyzing samples, by weight or sizeB. Mental skillsA.1 Understand the terminology related to gravimetric quantitative analysis, neutralization titrations, and sedimentationA.2 The ability to choose the appropriate chemical reaction for gravimetric quantitative analysis, neutralization titrations, and sedimentationA.3 The ability to perform all calculations related to quantitative, gravimetric and volumetric analysisA.4 The ability to express and discuss results A.5 The ability to select the optimal method for analysisT. Practical & professional skillsA.1 Identify the glass tools required for accurate quantitative gravimetric analysis and calibrationA.2 Identify the types of evidence needed for the types of chemical reactions used in the analysis.A.3 Learn how to prepare solutions and determine the masses of materials needed in the analysis.A.4 The ability to deal with errors in the results of the analysis A.5 Learn how to conduct experiments related to quantitative gravimetric analysis, neutralization titrations, and sedimentationw. Generic and transferable skillsA.1 The ability to discuss and work in an individual and independent manner, relying on personal skills of understanding and analysisA.2 Learn how to rationalize time while conducting the analysisA.3 The ability to perform mathematical calculations accurately and in a short timeA.4 The ability to prepare reports for presenting and discussing results A.5 Understand simple chemical analysis skills

Teaching and learning methods

1. Lectures 2 . exercises 3 . Duties

1. Course content(Course contents)

Scientific subject

The number of hours

a lecture

exercises

discussion

independent study

number of weeks

1. General introduction to analytical chemistry

i. Qualitative chemical analysis.

ii. Quantitative chemical analysis.

iii. Pre-analysis steps (how to pick and digest the sample).

iv. Choose the analysis method.

v. Accuracy and credibility.

vi. Types of errors (regular and random error).

vii. Methods of expressing concentrations (natural and chemical).

4

4

-

--

-

2

2. Weight quantitative analysis

i. Introduction to gravimetric quantitative analysis.

ii. Gravimetric analysis requirements and steps.

iii. Calculations based on gravimetric analysis.

iv. Weighing chemical coefficient.

v. Problems and examples of gravimetric analysis methods.

6

6

-

--

-

3

3. Volumetric quantitative analysis.

i. Calibration.

ii. Types of reactions used in volumetric quantitative analysis.

iii. Calibration curve.

iv. Volumetric analysis calculations.

v. Equivalent weight in acidity and basicity reactions.

vi. Equivalent weight in redox reactions.

vii. Equivalent weight in precipitation reactions.

viii. Equivalent weight in complex formation reactions.

ix. Titration calculations using molar and molar concentration.

6

6

-

--

-

3

4. An introduction to equilibrium calibrations.

i. Ionization of acids and bases in aqueous media.

ii. Acidity of aqueous solutions and pH.

iii. Calculating the pH of solutions of strong acids and bases.

iv. Calculating the pH of solutions of weak acids and bases.

v. Calculate the pH of salt solutions.

vi. Calculate the pH of buffer solutions.

vii. buffer solution capacity.

viii. The mechanism of action of the buffer solution.

ix. Calculate the change in pH during neutralization titrations.

4

4

-

--

-

2

5. Equivalent calibration curves and guides.

i. Titration of a strong acid with a strong base and vice versa.

ii. Titration of a weak acid with a strong base.

iii. Titration of a weak base with a strong acid.

iv. Evidence in tie titrations.

v. Ionization and its relationship to change the color of the guide.

vi. Factors affecting the color change of the guide.

vii. Examples of some visual evidence in equilibrium calibrations.

viii. Accuracy of equalization calibrations.

ix. Applications of neutralization titrations in aqueous media.

4

4

-

--

-

2

6. sedimentation titrations.

i. Theoretical foundations of sedimentation.

ii. Saturation and supersaturation phases.

iii. Factors affecting the formation of the precipitate and its solubility.

iv. Molar solubility and solubility product constant.

v. Calculations of solubility and solubility constant

vi. Sedimentation calibration curve.

vii. Factors affecting the calibration curve.

viii. Sedimentation titration applications.

4

4

-

--

-

2

(References)

References address

publisher

Release

Author

where it is located

Prescribed textbooks

Fundamental of Analytical Chemistry

Brooks

9th edition

Skook west and F. James Holler

Free Book online

Help books

Volumetric and gravimetric analysis book

Tripoli University

Dr. Mahmoud Al-Rayes and Dr. Amr Qoliza

University sales

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