CH311 : Analytical Chemistry(III)

Department

Department of Chemistry

Academic Program

Bachelor in Chemistry

Type

Compulsory

Credits

Prerequisite

CH212

Overview

The course aims to introduce the student to the following:• Knowledge of the theoretical foundations and principles of automated chromatographic analysis• Knowledge of the theoretical foundations and principles of automated spectral analysis of devices such as GC, HPLC, EP• Knowledge of theoretical calculations related to the work of these devices• Knowledge of theoretical calculations related to the work of these devices

Intended learning outcomes

a. Knowledge & understandingA.1 The student will be familiar with the theoretical foundations and principles of the instrumental analysis by chromatographic methodsA.2 The ability to solve mathematical problems related to the work of these methodsA.3 Know the special applications of each method in qualitative and quantitative analysis and how to deal with themA.4 The student is familiar with the quality methods and standard criteria for the different methods of separation and the use of Microsoft Excel in analyzing the results of the obtained experiments.A.5 The student will know how to operate GC, HPLCB. Mental skillsB.1 Analyze problems and apply technical solutions for chromatographic separation methodsB.2 Compare the different chapters in environmental analysisB.3 Acquaintance with green chromatographic analysis methodsB.4 Participation in the research activity of the devicesB.5 Identifying defects and interferences related to the analysis of the devices, analyzing the results and handling errorsT. Practical & professional skillsC.1 Using some methods of chromatographic analysis in analyzing real samplesC.2 Designing practical experiments using GC, HPLC devicesC.3 Choose the appropriate separation method for the type of analysis in the laboratoryC.4 The ability to operate and maintain the equipmentC.5 The ability to use mathematical and statistical methods to analyze the results obtained from these methods and the skill of using ISO in setting and operating devicesw. Generic and transferable skillsD.1 presents the information and explains the work and installation of the equipment orally and in writingD.2 Using appropriate techniques for chromatographic analysis and other separation methods in analyzing real samplesD.3 Work in an individual and independent manner, relying on personal skills of understanding and analysisD.4 Discussion in a scientific mannerD.5 Be able to present data, write reports in sound scientific language, and acquire skills in operating devices

Teaching and learning methods

Lectures 2 . exercises 3 . Duties 4. Periodic tests 5. Panel discussions 6. Visits to specialized research centers

Methods of assessments

First written exam 25%Second written exam 25%final exam 50%

1. محتوى المقرر (Course contents)

الموضوع العلمي	عدد الساعات	محاضرة	تمارين	مذاكرة مستقلة	عدد الأسابيع
Theory of chromatographic separations Solvent Extraction Theory What Is the Chromatographic Process Chromatography in More than One Dimension -Visualization of the Chromatographic Process at the Molecular Level: Analogy to Basic Equations Describing Chromatographic Separation, How Do Column Variables Affect Efficiency (Plate Height) - Practical Optimization of Chromatographic Separations Qualitative Chromatography: Analyte Identification Quantitative Measurements in Chromatography- Peak Area or Peak Height: What Is Best for Quantitation Calibration with an External Standard Calibration with an Internal Standard Examples of Chromatographic Calculations Ion Exchange Chromatography Size Exclusion chromatography Paper chromatography Affinity chromatography	8	4	-	-	4
Gas Chromatography Historical Development of GC: The First Chromatographic Instrumentation Advances in GC Leading to Present-Day Instrumentation GC Instrument Component Design (Injectors) Syringes. Autosamplers SPME, Split Injections Splitless Injections GC Instrument Component Design (the Column) Column Stationary Phase Selecting a Stationary Phase for an Application Effects of Mobile Phase Choice and Flow Parameter- GC Instrument Component Design (Detectors)	8	4	-	-	4
High-Performance Liquid Chromatography HPLC Column and Stationary Phase Support Particle Considerations Stationary-Phase Considerations. Chiral Phases for Separation of Enantiomers Effects on Separation of Composition of the Mobile Phase-New HPLC-Phase Combinations Ion-Exchange Chromatography. HPLC Detector Design and Operation Interfacing HPLC to Mass Spectrometry Applications of HPLC	8	4	-	-	4
Electrophoresis Capillary Zone Electrophoresis (CZE) Sample Injection in CZE Capillary Electrochromatography Micellar Electrokinetic Capillary Chromatography Planar Chromatography and Planar Electrophoresis Column Technology for Capillary Electrochromatography	4	2	-	-	2

1. the reviewer (References)

References title	publisher	Release	Author	Her whereabouts
Chromatography: Concepts and Contrasts,	Wiley	2nd edition	James M. Millerr	Internet
Advances in chromatography	CRC	Volume 65	Fli	Science Library - Internet
Undergraduate Instrumental Analysis	CRC Press	7th edition	James W. Robinson, Eileen Skelly Frame, George M. Frame II	Science Library - Internet

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Arabic language 1 (AR051)
General Physics І (Electricity ) (PH110)
General Chemistry 1 (CH101)
Mathematics 1 (MA100)
English Language 1 (EL101)
Principles of Atmospheric Science (AT112)
General Physics 2 (PH112)
General chemistry 2 (CH102)
General Chemistry 2 Laboratory (CH103)
Calculus and Analysis principle 2 (MA102)
Organic chemistry I (CH231)
Thermodynamics and Gases (CH241)
Ordinary Differential Equations (MA201)
Fundamentals of Inorganic Chemistry (CH221)
Analytical Chemistry(I) (CH211)
Practical Analytical Chemistry (CH213)
Methods for preparing inorganic compounds I (practical) (CH223)
Organic chemistry II (CH232)
Practical Analytical Chemistry, (CH214)
Thermodynamics and solutions (CH242)
Chemistry of Main Group Elements (CH222)
Analytical Chemistry(II) (CH212)
English language 2 (EL102)
Practical Analytical Chemistry (III) (CH013)
Organic chemistry Practical (CH031)
Industrial Chemistry (CH461)
Electrochemistry (CH341)
Thermodynamics and Solutions Lab (CH243)
Analytical Chemistry(III) (CH311)
Fundamentals of transition elements (CH321)
organic chemistry 3 (CH331)
Practical Industrial chemistry I (CH463)
Practical Analytical Chemistry(IV) (CH014)
Analytical Chemistry(IV) (CH312)
Transition elements chemistry studies (CH322)
Organic chemistry III Practical (CH333)
Biochemistry (CH451)
Organic chemistry IV (CH332)
Quantum chemistry (CH342)
Electrochemistry Lab (CH345)
Biochemistry lab I (CH453)
Molecular Spectroscopy (CH343)
Organic chemistry IV Practical (CH033)
Solid State Chemistry (CH344)
Practical Analytical Chemistry(V), (CH414)
Organometallic Chemistry (CH421)
Preparation and Methods for detection of inorganic compounds (CH424)
Industrial Chemistry (II) (CH462)
Analytical Chemistry(V) (CH441)
Nuclear chemistry (CH323)
Industrial Chemistry (II) Lab (CH464)
Kinetic Chemistry lab (CH043)
Kinetic Chemistry (CH442)