CH424 : Preparation and Methods for detection of inorganic compounds

Department

Department of Chemistry

Academic Program

Bachelor in Chemistry

Type

Compulsory

Credits

03

Prerequisite

CH321

Overview

• Develop students' skills in preparing and working in an inert atmosphere or using materials that are sensitive to atmospheric air• Preparation of some tetrahedral complexes, planar square and octahedral complexes are selected• Purification and identification of complexes prepared using volumetric and gravimetric analysis and spectroscopic devices• Helps to improve the skill of writing scientific reports for experiments

Intended learning outcomes

a. Knowledge & understandingA.1 The student has knowledge of the general methods of preparing complexesA.2 The student has concepts about the reasons for the stability or dissociation of complexes prepared with different factorsA.3 The student has a lot of knowledge about the use of scientific theories to identify some properties of complex preparationsA.4 The student will have many concepts about the use of prediction of potential mechanisms in inorganic reactionsB. Mental skillsB.1 The student acquires the skill of choosing the appropriate method for the gravimetric and volumetric analysis of a complex, according to the complex to be preparedB.2 The student acquires the skill of identifying the reasons for the stability or dissolution of the prepared complexesB.3 The student acquires the skill of interpreting the results obtained from the analyzes of the complexB.4 The student acquires the skill of interpreting the spectra of the prepared complexes and choosing the appropriate method for preparing a compoundT. Practical & professional skillsC.1 The student should have the ability to determine the appropriate methods for preparing complexesC.2 The student should possess the skill of preparing and purifying the prepared compoundsC.3 The student should possess the skill of analyzing the prepared complexesC.4 The student should have the skill of interpreting the spectra of the prepared complexesw. Generic and transferable skillsD.1 The student acquires the skill of using laboratory equipment and analysis equipmentD.2 The student acquires the skill of organized group workD.3 The student acquires the skill of writing practical reportsD.4 The student acquires a skill in measuring the percentage of presence of elements, whether natural or prepared

Teaching and learning methods

• Giving lectures• solving exercises• Panel discussions• Homework, reports and the formation of discussion groups

Methods of assessments

First written exam 25%Second written exam 25%final exam 50%

1. محتوى المقرر (Course contents)

الموضوع العلمي

عدد الساعات

محاضرة

معمل

تمارين

مناقشة

مذاكرة مستقلة

عدد الاسابيع

The preparation and chemical analysis of Ferrous oxalatedihydrate:

FeC2O4.2H2O

6

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6

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1

The preparation and chemical analysis of Potassium trioxalatoferrate(III) Hydrate:

K3[Fe(C2O4)3]3H2O

6

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6

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1

preparation and chemical analysis of Trithioureacupper(I) sulphate hydrate:

[Cu(tu)3]2SO4.3H2O

6

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6

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1

The preparation and chemical analysis of Cis-Potassium diaquadioxalatochromate(III) hydrate:

Cis-K[Cr(C2O4)2(H2O)2].2H2O

6

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6

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1

The preparation and chemical analysis of Trans-Potassium diaquadioxalatochromate(III) hydrate: Cis-K[Cr(C2O4)2(H2O)2].2H2O

6

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6

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1

The preparation and chemical analysis of Bis-acetylacetonatocopper(II):

Cu(acac)2

6

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6

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1

The preparation and chemical analysis of VanadylAcetylacetonate and Adduct with Pyridine:

I. [VO(acac)2] II. C5H5N (py)

6

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6

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1

The preparation and chemical analysis of Bis-acetylacetonatodiaquacobalt(II): Co(acac)2(H2O)2

6

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6

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1

The preparation and determination of the composition of iron-phenanthroline complex by Job’s method:

[Fe(1,10-O.Phen)3]2+

6

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6

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1

The preparation and chemical analysis of Dicyanoamminenickel(II) clathrate:

Ni(CN)2NH3

6

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6

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1

The preparation and chemical analysis of Schiff bases and with its metal complexes:

(H2salphen) and [ Cu(salphen) ]

6

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6

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1

The preparation and chemical analysis of Xanthate complexes : Ni(ROCS2)2 and Ni(ROCS2)3

6

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6

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1

Preparation of Organometallic compound of ruthenium

CpRu(PPh3)2Cl ( Cp= η5-C5H5) or

6

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6

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1

Preparation of Hydrido and chelate compound of cobalt

HCo(P(OPh)3)4

6

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6

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1

Introduction to Atmospheric Science (AT111)
Arabic language 1 (AR051)
General Physics І (Electricity ) (PH110)
General Chemistry 1 (CH101)
Mathematics 1 (MA100)
English Language 1 (EL101)
Principles of Atmospheric Science (AT112)
General Physics 2 (PH112)
General chemistry 2 (CH102)
General Chemistry 2 Laboratory (CH103)
Calculus and Analysis principle 2 (MA102)
Organic chemistry I (CH231)
Thermodynamics and Gases (CH241)
Ordinary Differential Equations (MA201)
Fundamentals of Inorganic Chemistry (CH221)
Analytical Chemistry(I) (CH211)
Practical Analytical Chemistry (CH213)
Methods for preparing inorganic compounds I (practical) (CH223)
Organic chemistry II (CH232)
Practical Analytical Chemistry, (CH214)
Thermodynamics and solutions (CH242)
Chemistry of Main Group Elements (CH222)
Analytical Chemistry(II) (CH212)
English language 2 (EL102)
Practical Analytical Chemistry (III) (CH013)
Organic chemistry Practical (CH031)
Industrial Chemistry (CH461)
Electrochemistry (CH341)
Thermodynamics and Solutions Lab (CH243)
Analytical Chemistry(III) (CH311)
Fundamentals of transition elements (CH321)
organic chemistry 3 (CH331)
Practical Industrial chemistry I (CH463)
Practical Analytical Chemistry(IV) (CH014)
Analytical Chemistry(IV) (CH312)
Transition elements chemistry studies (CH322)
Organic chemistry III Practical (CH333)
Biochemistry (CH451)
Organic chemistry IV (CH332)
Quantum chemistry (CH342)
Electrochemistry Lab (CH345)
Biochemistry lab I (CH453)
Molecular Spectroscopy (CH343)
Organic chemistry IV Practical (CH033)
Solid State Chemistry (CH344)
Practical Analytical Chemistry(V), (CH414)
Organometallic Chemistry (CH421)
Preparation and Methods for detection of inorganic compounds (CH424)
Industrial Chemistry (II) (CH462)
Analytical Chemistry(V) (CH441)
Nuclear chemistry (CH323)
Industrial Chemistry (II) Lab (CH464)
Kinetic Chemistry lab (CH043)
Kinetic Chemistry (CH442)