CH311P : Analytical chemistry 3 practical

Department

Department of Chemistry

Academic Program

Bachelor in Chemistry

Type

Compulsory

Credits

01

Prerequisite

CH331.

Overview

This course is concerned with training the student to conduct a set of experiments:

1- Theoretical explanation on the use of some simple equipment and techniques such as solvent separation, electrolysis and spectroscopy.

2- Experiments in electrical measurements, serum pH measurement and control of related equipment.

3- Determination of the concentration of some metals using a spectroscopy (UV-Visible).

4- Perform some measurements using paper chromatography and thin layer chromatography.

5- Using ion exchange columns in purifying solutions and making measurements before and after separation.

6- Use of separation by organic solvent extraction technique and measurements after separation.

7- Using a flame spectrometer to measure the concentration of some metals such as Na & K.

8- Conducting some experiments on measuring electrical conductivity and determining the concentration of some acid solutions such as hydrochloric acid and acetic acid, and a mixture of them.

9- Measurement of total dissolved salts in water TDS based on conductivity measurement.

Intended learning outcomes

At the end of the course, the student will be able to:

1. Discusses the nature and danger of chemicals.

2. Coercion and analyze the reasons for choosing the appropriate method for the preparation of chemical solutions.

3. Analyzes the results of experiments.

4. Discover how important it is for the results of the analyzes to be compatible with realistic values.

5. Identify the sensitivity of devices and methods used dilution coefficient.

6. Writes reports on the results of chemical analyzes accurately and skillfully.

7. Uses appropriate methods to perform analysis of a particular substance.

8. Uses international specifications and compare their analysis methods.

9. Employs his knowledge of methods of determining the quality of industrial products.

10. Learns how to present analysis results supported by statistical analysis.

11. Has a team spirit and respects the opinions of his colleagues. 12. Self-learning and continuous learning ability.

13. Critical and creative thinking and problem solving are used when conducting laboratory experiments.

14. Respects professional ethics.

15. Employ his knowledge in presenting the results and writing the report well.

16. Recognize how to deal with materials and equipment within the laboratory.

17. Determines how devices are used and calibrated.

18. Multiple methods of preparing different solutions.

19. Demonstrates how to handle samples during analysis.

20. Explains how to find the appropriate way to perform a particular analysis.

Teaching and learning methods

1- Explanation of the required experiments on the board.

2- Granting the student, a commitment to all the required experiments and methods of preparing solutions.

3- Laboratory activities and data collection.

4- Real-time follow-up during experiments to ensure that each student is able to use the tools correctly.

Methods of assessments

Notes

Percentage

Evaluation weight

Evaluation duration

Evaluation methods

No.

15%

15

Fifth week

First written test (multiple choice style and essay questions)

1

15%

15

Tenth week

First written test (multiple choice style and essay questions)

2

10%

10

During term

Reports on the experiments

3

10%

10

During term

Attendance and experiments conductance

4

50%

50

Last week

Final Exam

5

Course Content

Week

Scientific topic

Teaching hours

Lectures

Exercises

Discussion

1

Theoretical explanation on the use of some simple equipment and techniques such as solvent separation, electrolysis and spectroscopy.

3

2

Experiments in electrometric, measurements of pH and conductivity and control of related equipment

3

3-4

Determination of the concentration of some metals using a spectroscopy (UV-Visible)

6

5

First med term exam

6

Perform some measurements using paper chromatography and thin layer chromatography

3

7

Using ion exchange columns to purify solutions and make measurements before and after separation

3

8-9

Use of separation by organic solvent extraction technique and measurements after separation

6

10

Second med term exam

11-12

Using a flame spectrometer to measure the concentration of some metals such as Na & K

6

13

Conducting some experiments on measuring electrical conductivity and determining the concentration of some acid solutions such as hydrochloric acid and acetic acid, and a mixture of them.

3

14

Measurement of Total Dissolved Salts in Water TDS Based on Conductivity Measurement

3

15

Final exam

Total

36

References

Reference Title

Publisher

Version

The author

Reference location

Rapporteur notes

Course Professor

Faculty photographer

Foundations of Practical Analytical Chemistry

(Arabic Edition)

1st edition

Ragiab Issa & Farag Shtiwi

Public laboraories

Quranic Studies 1 (AR101)
Principles of statistics (ST100)
Fundamentals of Education (EPSY101)
General Psychology (EPSY 100)
General Chemistry I (.CH101)
Arabic language 1 (AR103)
Arabic language 2 (AR104)
computer 1 (CS100)
General English1 (EN100)
General Teaching Methods (EPSY 201)
Developmental Psychology (EPSY 203)
Quranic studies2 (AR102)
General Mathematics 1 (MM111)
General chemistry II practical (CH102P.)
General chemistry II (CH102.)
Basics Of Curriculums (EPSY 202)
Educational Psychology (EPSY 200)
Computer 2 (CS101)
Arabic language 3 (AR105)
Physical Chemistry I (CH241.)
Analytical Chemistry I (CH211.)
Organic chemistry 1 (CH231.)
Inorganic Chemistry I (CH221.)
Organic Chemistry 2 (CH232.)
Physical Chemistry 2 (CH242.)
Methods of teaching chemistry (CH201)
General Mathematics 2 (MM112)
Research Methods (EPSY301)
Measurements and Evaluation (EPSY 302)
Analytical Chemistry 2 (CH212.)
Inorganic Chemistry II (CH222.)
Organic chemistry 1 Practical (CH231P.)
Physical chemistry 1 Practical (CH241P.)
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Analytical chemistry 3 (CH311.)
Inorganic chemistry 3 (CH321.)
Organic chemistry 3 (CH331.)
Physical chemistry 3 (CH341.)
(CH212P.)
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Inorganic chemistry 2 practical (CH321P.)
Inorganic chemistry 4 (CH322.)
Organic chemistry 2 practical (CH331P)
Organic chemistry 4 (CH332.)
Organic chemistry 3 practical (CH332P)
Physical chemistry 2 practical (CH341P.)
Physical chemistry 4 (CH342.)
Physical Chemistry 3 practical (CH342P)
Physical chemistry 5 (CH343.)
Inorganic chemistry 3 practical (CH322P.)
Biochemistry (CH451)
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Teaching Practice (EPSY 402)
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